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Forensic Science International
Volume 157, Issue 1
, Pages 1-22
, 10 February 2006
Forensic applications of isotope ratio mass spectrometry—A review
References
- . Stable carbon isotopic composition of gasolines determined by isotope ratio monitoring gas chromatography mass spectrometry. Org. Geochem. 2002;33:149–159
- . Automated analysis of light-element stable isotopes by isotope ratio mass spectrometry. In: Boutton TW, Yamasaki S editor. Mass Spectrometry of Soils. New York: Marcel Dekker Inc; 1996;p. 1–46
- F. Fourel, Forensic Applications in Continuous Flow IRMS Using the IsoPrime. Presentation at the Forensic Isotope Ratio Mass Spectrometry (FIRMS) Conference, 16–17 September 2002 (http://www.forensic-isotopes.rdg.ac.uk/conf/conf.htm).
- . Putting the arsonist at the scene: “DNA” for the fire investigator? Gas chromatography/isotope ratio mass spectrometry. Fire Arson Invest. 2002;51(2):30–34
- . Kirk's Fire Investigation. 4th ed.. New Jersey: Brady Prentice Hall; 1997;p. 55
- . Forensic applications of isotope ratio mass spectrometry. In: Yinon J editors. Advances in Forensic Applications of Mass Spectrometry. USA: CRC Press; 2004;p. 149–180
- . Referencing strategies and techniques in stable isotope ratio analysis. Rapid Commun. Mass Sp. 2001;15:501–519
- Micromass Stable Isotope Standardisation Template. Chart no. CH20/DAM, Version 1, November 2000 (00/00329).
- . The Biomarker Guide Interpreting Molecular Fossils in Petroleum and Ancient Sediments. New Jersey: Prentice Hall; 1993;pp. 122–130
- . Continuous-flow stable isotope analysis for biologists. Spectroscopy. 1989;4(7):42–52
- . High precision isotope ratio monitoring techniques in mass spectrometry. J. Mass Spectrom. 1996;31:225–235
- J. Hoogewerff, Origin of Trace Element and Isotope Variation, Relevance for Forensic Studies. Presentation at the NITECRIME workshop, Wellington, New Zealand, 2 April 2004.
- . The Biological Fractionation of Isotopes. Florida: Academic Press; 1985;
- . Precise isotope ratio measurements as a unique tool in modern analytical chemistry. Anal. Bioanal. Chem. 2004;378:227–228
- . Isotope-abundance variations of selected elements (IUPAC Technical Report). Pure Appl. Chem. 2002;74(10):1987–2017
- . Compound-specific stable isotope analysis of organic contaminants in natural environments: a critical review of the state of the art, prospects, and future challenges. Anal. Bioanal. Chem. 2004;378:283–300
- . Isotopic analysis of 13C as a tool for comparison and origin assignment of seized heroin samples. J. Forensic Sci. 1997;42(3):429–433
- . Application of stable isotopes and radioisotopes in environmental forensics. In: Murphy BL, Morrison RD editor. Introduction to Environmental Forensics. China: Academic Press; 2002;p. 99–136
- Website: http://isohis.iaea.org/userupdate/description/Precip0.html
- . Carbon isotope pattern in purine alkaloids a key to isotope discriminations in C1 compounds. Phytochemistry. 1996;41(4):1073–1077
- . Geographic origin determination of heroin and cocaine using site-specific isotopic ratio deuterium NMR. J. Forensic Sci. 2000;45(3):552–562
- . Isotopic characterisation of 3,4-methylenedioxyamphetamine and 3,4-methylenedioxymethylamphetamine (ecstacy). Analyst. 2002;127:830–833
- . Review: applied gas chromatography coupled to isotope ratio mass spectrometry. J. Chromatogr. A. 1999;842:351–371
- . Gas chromatography with mass spectrometry or isotope-ratio mass spectrometry in studying the geographical origin of heroin. Anal. Chim. Acta. 1991;247:249–254
- . 15N isotopic analyses: a powerful tool to establish links between seized 3,4-methylenedioxymethamphetamine (MDMA) tablets. Anal. Bioanal. Chem. 2003;376:486–490
- . Proceedings: network developing forensic applications of stable isotope ratio mass spectrometry Conference 2002. Sci. Justice. 2003;43(3):153–160
- . 13C Isotopic analysis of an acetaminophen and diacetylmorphine mixture. J. Chromatogr. A. 1996;756:203–210
- . Amount-dependent isotopic fractionation during compound-specific isotope analysis. Rapid Commun. Mass Sp. 2003;17:970–977
- . Oxygen isotopes in nature and in the laboratory. Science. 1948;108:489–496
- ThermoFinnigan DELTAPlusXP Operating Manual. Ident. No. 114 90 80, Issue 06/2002.
- Micromass IsoPrime™ Solution Driven Stable Isotope Ratio Mass Spectrometry. Brochure No. BR39/DAM Version 1 March 2001.
- PDZ Europa 20-20 Series IRMS Product Information Sheet 02 Issue 1.1 Cat. No. 20401/3.
- Website: http://www.forensic-isotopes.rdg.ac.uk/techniq/techniq.htm
- Thermo Electron Corporation. Finnigan™ LC IsoLink Catalogue, 2003.
- . A new concept for isotope ratio monitoring liquid chromatography/mass spectrometry. Rapid Commun. Mass Sp. 2004;18:2260–2266
- . Rapid conversion of organic nitrogen to N2 for mass spectrometry: an automated Dumas procedure. Anal. Biochem. 1965;13:1–5
- . Interfacing an automatic elemental analyser with an isotope ratio mass spectrometer: the potential for fully automated total nitrogen and nitrogen-15 analysis. Analyst. 1983;108:971–977
- J. Oesselmann, A. Hilkert, C.B. Douthitt, Trends in stable isotope analyses and applications. ThermoFinnigan DeltaPlus MAT 252 Application Presentation, 2001.
- ThermoFinnigan ConFlo III Operating Manual. Ident. No. 111 0041, Issue 5/2001.
- ThermoFinnigan High Temperature Conversion Elemental Analyzer (TC/EA) Operating Manual. Ident. No. 112 76 01, Issue 11/2001.
- Micromass EA System The IRMS sample preparation device for Dumas combustion or pyrolysis of solids and liquids. Flyer No. FL56/DAM Version 2 May 2001.
- PDZ Europa Integra-CN 15N and 13C analyser Product Information Sheet 06 Issue 1 Cat. No. 20801.
- . Isotope-ratio–monitoring gas chromatography–mass spectrometry. Anal. Chem. 1978;50(11):1465–1473
- ThermoFinnigan High Temperature Conversion Interface (GC/TC) Operating Manual. Ident. No. 112 76 31, Issue 04/2001.
- ThermoFinnigan GC Combustion Interface III (GC/CIII) Operating Manual. Ident. No. 111 00 71, Issue 06/2002.
- Micromass GC System GC combustion and pyrolysis CF IRMS featuring ChromeHD™ technology. Flyer No. FL57/DAM Version 2 May 2001.
- PDZ Europa GC-CP-IRMS Interface Product Information Sheet 03 Issue 1 Cat. No. 10401/1.
- . Stable isotopic characterization of analgesic drugs. Pharm. Technol. 2004;60–67
- . Stable isotopic characterization of active pharmaceutical ingredients. J. Pharmaceut. Biomed. 2004;35(1):21–30
- . Determination of the Origin of Drugs by Measuring Natural Isotope Contents: D/H and 13C/12C Ratios of Some Diazepam Samples. Z. Naturforsch. 1976;31c:111–114
- In: Browne TR editors. Stable Isotopes in Pharmaceutical Research. Amsterdam: Elsevier Science; 1997;
- . Determination of carbon-13 content of sugars of fruit and vegetable juices. Anal. Chim. Acta. 1993;271:31–38
- Micromass Application Note 503 1999. GC–IRMS Detection of Adulterated Chamomile Extracts.
- Micromass Application Note 502 1999. The use of GC–C–IRMS in the Detection of Adulterated Vanilla Bean Extracts.
- J. Morrison, F. Fourel, Application of 13C EA/IRMS to the detection of adulteration of honey. Micromass Application Brief AB8, 1999.
- M. Boner, H. Forstel, Examination of the 13C/12C Isotopes in Sparkling and Semi-sparkling Wine with the Aid of Simple On-line Sampling. Micromass Application Note 516, 2002.
- J. Lofthouse, C. Rhodes, K. Heaton, C. Burwood, P. Brereton, S. Hird, The use of pyrolysis-isotope ratio mass spectrometry (Py-IRMS) to Combat Fraud in the food industry: some lessons to be learnt for applications in forensics. Poster at the Forensic Isotope Ratio Mass Spectrometry (FIRMS) Conference, 16–17 September 2002 (http://www.forensic-isotopes.rdg.ac.uk/conf/conf.htm).
- S. Kelly, J. Hoogewerff, Detection of Food Adulteration. Presentation at the NITECRIME workshop, Wellington, New Zealand, 2 April 2004.
- . Carbon isotopes in vanillin and the detection of falsified “natural” vanillin. J. Agric. Food Chem. 1983;31:1265–1268
- . Detection of fraudulent vanillin labelled with 13C in the carbonyl carbon. J. Agric. Food Chem. 1985;33(3):323–325
- . Isotopic composition of carbon in apple juice. J. Agric. Food Chem. 1980;28:362–364
- . Characterization of European wine glycerol: stable carbon isotope approach. J. Agric. Food Chem. 2004;52:5902–5906
- . Determination of the C-13/C-12 ratio of ethanol derived from fruit juices and maple syrup by isotope ratio mass spectrometry: collaborative study. J. AOAC Int. 2004;87(3):621–631
- . Determination of H-2/H-1 and C-13/C-12 isotope ratios of (E)-methyl cinnamate from different sources using isotope ratio mass spectrometry. J. Agric. Food Chem. 2004;52(10):3065–3068
- . Application of isotope ratio monitoring gas chromatography–mass spectrometry to the analysis of organic residues of archaeological origin. Analyst. 1994;119:909–914
- . Single-compound isotopic analysis of organic materials in archaeology. LC GC N. Am. 2004;22(11):1098
- . Use of table chlorine and carbon isotope analysis in environmental forensic investigations of groundwater contamination. In: Abstracts from PITTCON – Analytical Chemistry and Applied Spectroscopy Conference. Chicago, USA. 7–12 March 2004;
- F. Fourel, T. Merren, J. Morrison, L. Wassenaar, K. Hobson, Application of EA Pyrolysis – IRMS δD and δ18O Analysis to Animal Migration Patterns. Micromass Application Note 511, 2000.
- T. Merren, J. Morrison, S. Dudd, K. Hobson, L. Wassenaar, Investigation of Whale Migration Patterns using Stable Isotope Variations in Baleen Growth Bands. Micromass Application Note 515, 2001.
- . The role of species abundance in determining breeding origins of migratory birds with stable isotopes. Ecol. Appl. 2004;14(6):1780–1788
- M.A. Stelling, G.J.Q. Van der Peijl, Forensic methods for criminal investigations related to endangered species. Netherlands Forensic Institute report, December 2001.
- . Characterisation of animal products according to geographic origin and feeding diet using nuclear magnetic resonance and isotope ratio mass spectrometry. Part II. Beef meat. Food Chem. 2004;86:251–256
- . Characterisation of animal products according to geographic origin and feeding diet using nuclear magnetic resonance and isotope ratio mass spectrometry: cow milk. Food Chem. 2004;85:63–66
- . Stable isotope variation as a tool to trace the authenticity of beef. Anal. Bioanal. Chem. 2004;378:301–310
- . Characterisation of the geographical origin of buffalo milk and mozzarella cheese by means of analytical and spectroscopic determinations. Food Chem. 2005;89:139–147
- S.A. Phillips, S. Doyle, S. Mountford, Proceedings of the Forensic Isotope Ratio Mass Spectrometry (FIRMS) Workshop, 14 May 2003 (http://www.forensic-isotopes.rdg.ac.uk/papers/workshop.pdf).
- Finnigan Mat, 15N/14N and 13C/12C by EA/IRMS Forensic Studies Using the ConFlo II Interface. Application Flash Report No. 15. 12/1995 PL 0/1177.
- K. Pye, Isotopic and trace element characterization of human teeth and bones for identification and provenance purposes. Presentation at the NITECRIME workshop, Wellington, New Zealand, 2nd April 2004.
- H.W. Kreuzer-Martin, M.J. Lott, J.R. Ehleringer, Locating the Geographic Origin of Microbial Cultures Through Stable Isotope Ratio Analysis. Poster at the Forensic Isotope Ratio Mass Spectrometry (FIRMS) Conference, 16–17 September 2002 (http://www.forensic-isotopes.rdg.ac.uk/conf/conf.htm).
- . Stable Isotope Ratios as a Tool in Microbial Forensics-Part 1. Microbial Isotopic Composition as a Function of Growth Medium. J. Forensic Sci. 2004;49(5):954–960
- . Stable isotope ratios as a tool in microbial forensics. Part 2. Isotopic variation among different growth media as a tool for sourcing origins of bacterial cells and spores. J. Forensic Sci. 2004;49(5):1–7
- . Technical note: stable-isotope fingerprints of biological agents as forensic tools. J. Forensic Sci. 2003;48(1):1–5
- . Stable isotope (C-13, N-15 and S-34) analysis of the hair of modern humans and their domestic animals. Rapid Commun. Mass Sp. 2002;16(23):2195–2200
- . The potential use of continuous-flow isotope-ratio mass spectrometry as a tool in forensic soil analysis: a preliminary report. Rapid Commun. Mass Sp. 2003;17(23):2581–2584
- T. Ohuchi, K. Muehlenbachs, Isotopic fingerprinting of market products: carbon and hydrogen isotope ratios of polymer materials. Proceedings from the Canadian Society of Forensic Science (CSFS) 50th Anniversary Meeting Vancouver BC, 25–29 March 2003.
- . Forensic isotope ratio mass spectrometry of packaging tapes. Analyst. 2004;129:1206–1210
- . Isotopic and other investigations in relation to a safe burglary. In: Proceedings of the 17th International Symposium on the Forensic Sciences Handbook and Programme. Wellington, New Zealand, 28 March–2 April. 2004;
- . Multielement isotope analysis on drugs of abuse. Possibility for their origin assignment. Isot. Environ. Health S. 1996;32:226–228
- . Geo-location of heroin and cocaine by stable isotope ratios. Forensic Sci. Int. 1999;106:27–35
- . Chemical profiling of illicit heroin samples. Forensic Sci. Rev. 1999;11(2):106–119
- . Tracing the geographical origin of cocaine. Nature. 2000;408:311–312
- . Technical note: possible characterization of samples of Cannabis sativa L. by their carbon isotopic distributions. J. Forensic Sci. 1979;24:814–816
- . Natural abundance of stable carbon and nitrogen isotopes in Cannabis sativa reflects growth conditions. Aust. J. Plant Physiol. 2001;28:1005–1012
- FIRMS (Forensic Isotope Ratio Mass Spectrometry) Newsletter Volume 1, Issue 3, August 2003.
- M.J. Lott, J. Howa, J.R. Ehleringer, J.F. Jauregui, C. Douthitt, Detecting the Manufacturing Origins of Pseudoephedrines Through Stable Isotope Ratio Analysis, Poster at the Forensic Isotope Ratio Mass Spectrometry (FIRMS) Conference, 16–17 September 2002 (http://www.forensic-isotopes.rdg.ac.uk/conf/conf.htm).
- . Technical note: determination of ‘common-batch’ members in a set of confiscated 3,4-(methylendioxy)-methylamphetamine samples by measuring the natural isotope abundance: a preliminary study. Forensic Sci. Int. 1995;71:225–231
- F. Palhol, M. Chabrillat, N. Naulet, F. Fourel, S. Dudd, Tracking the Origin of Illicit MDMA Using 15N/14N Stable Isotope Ratios. Micromass Application Note 514, 2002.
- . N-15/N-14 isotopic ratio and statistical analysis: an efficient way of linking seized ecstasy. Anal. Chim. Acta. 2004;510:1–8
- . Determination of origin of ephedrine used as precursor for illicit methamphetamine by carbon and nitrogen stable isotope ratio analysis. Anal. Chem. 2004;76:4233–4236
- . 15N/14N isotopic ratio and statistical analysis: an efficient way of linking seized Ecstasy tablets. Anal. Chim. Acta. 2004;510:1–8
- . Improved method of detection of testosterone abuse by gas chromatography/combustion/isotope ratio mass spectrometry analysis of urinary steroids. J. Mass Spectrom. 1996;31(2):169–176
- A. Phillips, Gas chromatography combustion isotope ratio mass spectrometry for confirming testosterone administration from urinary androstanediols, Micromass Application Note 501, 1999.
- . Confirming testosterone administration by isotope ratio mass spectrometric analysis of urinary androstanediols. Steroids. 1997;62:379–387
- . Searching for new markers of endogenous steroid administration in athletes: “looking outside the metabolic box”. Forensic Sci. Int. 2004;143:103–114
- . Urinary analysis of 16(5α)-andronsten-3α-ol by gas chromatography/combustion/isotope ratio mass spectrometry: implications in anti-doping analysis. J. Chromatogr. B. 2004;810:157–164
- . Detection of exogenous hydrocortisone in horse urine by gas chromatography–combustion-carbon isotope ratio mass spectrometry. J. Chromatogr. B. 1997;702:85–91
- J.P. Jasper, J.S. Edwards, L.C. Ford, A Novel Method for Arson Accelerant Analysis: Gas Chromatography/Isotope Ratio Mass Spectrometry, 2001, Website: http://www.molecularisotopes.com/asia.html.
- P.M.L. Sandercock, Forensic comparison of unevaporated and evaporated automotive gasoline samples from Australia and New Zealand. Thesis submitted for the Degree of Doctor of Philosophy (Science) University of Technology, Sydney, December 2002.
- . Characterisation of refractory wastes at hydrocarbon-contaminated sites-II. Screening of reference oils by stable carbon isotope fingerprinting. Environ. Pollut. 1996;94(2):195–203
- . Forensic environmental geochemistry: differentiation of fuel types, their sources and release time. Org. Geochem. 1997;27:289–317
- . Concentrations and stable isotope values of btex in gasoline-contaminated groundwater. Environ. Sci. Technol. 1997;31:2469–2472
- . Tracing organic contaminants in groundwater: a new methodology using compound-specific isotopic analysis. Environ. Sci. Technol. 1997;31(11):3193–3197
- . Carbon isotope systematics of monoaromatic hydrocarbons: vaporization and adsorption experiments. Org. Geochem. 1999;30:765–775
- E.J.M. Diegor, T. Abrajano, L. Stehmeier, T. Patel, L. Winsor, Proceedings of the 19th International Meeting on Organic Geochemistry, Istanbul, Turkey, 1999. extended abstract only, abstract No. 010A, p.29, Abstracts published by TUBITAK Marmara Research Centre, Gebze-Kocaeli, Turkey (cited).
- . Carbon isotope fractionation during anaerobic biodegradation of toluene: implications for intrinsic bioremediation. Environ. Sci. Technol. 2000;34:892–896
- . Source identification of oil spills based on the isotopic composition of individual components in weathered oil samples. Environ. Sci. Technol. 1997;31:3417–3425
- . Molecular and isotopic analysis of oils by solid phase microextraction of gasoline range hydrocarbons. Org. Geochem. 1999;30:721–737
- . Detection of petroleum contamination in river sediments from Quebec City region using GC–IRMS. Org. Geochem. 1999;30:1559–1569
- . Review: oil spill identification. J. Chromatogr. A. 1999;843:369–411
- J.P. Jasper, J.S. Edwards, L.C. Ford, R.A. Corry, An Initial Report of the Arson Stable-Isotope Analysis Project, Poster at the Forensic Isotope Ratio Mass Spectrometry (FIRMS) Conference, 16–17 September 2002 (http://www.forensic-isotopes.rdg.ac.uk/conf/conf.htm).
- . The use of stable isotopes to differentiate specific source markers for MTBE. Environ. Forensics. 2001;2:215–221
- . The use of the isotopic composition of individual compounds for correlating spilled oils and refined products in the environment with suspected sources. Environ. Forensics. 2002;3:341–348
- . Hydrogen isotopic composition of individual n-alkanes as an intrinsic tracer for bioremediation and source identification of petroleum contamination. Environ. Sci. Technol. 2002;36:724–728
- . Classification of Duvernay sourced oils from central and southern Alberta using Compound Specific Isotope Correlation (CSIC). B. Can. Petrol. Geol. 2003;51(2):99–125
- . The distribution of natural stable isotopes of carbon as a possible tool for the differentiation of samples of TNT. J. Forensic Sci. 1975;20:455–459
- . Application of stable isotope ratios to the analysis of explosive residues. In: Proceedings of the Fifth International Symposium on the Analysis and Detection of Explosives. Washington, DC, 4–8 December. 1995;
- D. Wakelin, Isotopic ratio analysis of explosives traces – a new type of evidence, United Kingdom Defence Evaluation and Research Agency report DERA/CES/CS/CR000294, December 2000.
- D. Wakelin, Isotopic ratio analysis of explosives traces – a new type of evidence Part 2, United Kingdom Defence Evaluation and Research Agency report DERA/DSTL/CR00569, April 2001.
- A.M. Beardah, Stable isotope ratio mass spectrometry of explosives – a new type of evidence (Part 3), United Kingdom Defence Science and Technology Laboratory report DSTL/CR05104, October 2002.
- M.J. Lott, J. Howa, J.R. Ehleringer, Locating the origins of explosives through stable isotope ratio analysis, Poster at the Forensic Isotope Ratio Mass Spectrometry (FIRMS) Conference, 16–17 September 2002 (http://www.forensic-isotopes.rdg.ac.uk/conf/conf.htm).
- . The analysis of explosives and ignitable liquids using isotope ratio mass spectrometry. In: Proceedings of the 17th International Symposium on the Forensic Sciences Handbook and Programme. Wellington, New Zealand, 28 March–2 April. 2004;
PII: S0379-0738(05)00172-6
doi: 10.1016/j.forsciint.2005.03.012
© 2005 Elsevier Ireland Ltd. All rights reserved.
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Forensic Science International
Volume 157, Issue 1
, Pages 1-22
, 10 February 2006
